Motorola LS6000B-U Guide de l'utilisateur

TM247971-FJune 2005Beckman Coulter, Inc.4300 North Harbor Boulevard, Fullerton, CA 92834-3100©Copyright 2005 Beckman Coulter, Inc.Printed in U.S.A.LS

LS 6000 Scintillation System User’s ManualPN 247971-F 5-22 Data CalculationSingle Photon MonitoringCount Time per Data PointThis feature allows you to

LS 6000 Scintillation System User’s ManualPN 247971-F 5-23Data CalculationSingle Photon Monitoring5starts the elapsed time before the sample count is

LS 6000 Scintillation System User’s ManualPN 247971-F 5-24 Data CalculationSingle Photon Monitoring

LS 6000 Scintillation System User’s ManualPN 247971-F 6-1Isotope/DPM LibrariesThe Isotope Library66Isotope/DPM Libraries6.1 The Isotope LibraryIntrodu

LS 6000 Scintillation System User’s ManualPN 247971-F 6-2 Isotope/DPM LibrariesThe Isotope LibraryAccessing the Isotope LibraryTo use the Isotope Libr

LS 6000 Scintillation System User’s ManualPN 247971-F 6-3Isotope/DPM LibrariesThe Isotope Library62. Highlight “Print Isotope Library” and press SELEC

LS 6000 Scintillation System User’s ManualPN 247971-F 6-4 Isotope/DPM LibrariesThe Isotope LibraryAdding A New Isotope to the Isotope LibraryIsotopes

LS 6000 Scintillation System User’s ManualPN 247971-F 6-5Isotope/DPM LibrariesThe Isotope Library61. With the New Isotope Setup Menu displayed and “Sc

LS 6000 Scintillation System User’s ManualPN 247971-F 6-6 Isotope/DPM LibrariesThe Isotope LibraryNOTE The windows determined by Automatic Setup are

LS 6000 Scintillation System User’s ManualPN 247971-F 6-7Isotope/DPM LibrariesThe Isotope Library610. With both racks in position in the sample change

LS 6000 Scintillation System User’s ManualPN 247971-F 1-1IntroductionIntended Use11Introduction1.1 Intended UseThe Beckman LS 6720/6730/6750 Scintilla

LS 6000 Scintillation System User’s ManualPN 247971-F 6-8 Isotope/DPM LibrariesSetting Up A Quench Curve6.2 Setting Up A Quench CurveThe DPM LibraryTh

LS 6000 Scintillation System User’s ManualPN 247971-F 6-9Isotope/DPM LibrariesSetting Up A Quench Curve6standard set, refer to Counting the Standards

LS 6000 Scintillation System User’s ManualPN 247971-F 6-10 Isotope/DPM LibrariesSetting Up A Quench Curve5. If setting up quench curves for applicatio

LS 6000 Scintillation System User’s ManualPN 247971-F 6-11Isotope/DPM LibrariesSetting Up A Quench Curve68. Load the samples to count into the rear mo

LS 6000 Scintillation System User’s ManualPN 247971-F 6-12 Isotope/DPM LibrariesSetting Up A Quench Curvefrom the set and properly dispose of them. A

LS 6000 Scintillation System User’s ManualPN 247971-F 6-13Isotope/DPM LibrariesSetting Up A Quench Curve61. From the Main Menu, highlight “Isotope/DPM

LS 6000 Scintillation System User’s ManualPN 247971-F 6-14 Isotope/DPM LibrariesSetting Up A Quench CurveIf you do not wish to count a background quen

LS 6000 Scintillation System User’s ManualPN 247971-F 6-15Isotope/DPM LibrariesSetting Up A Quench Curve6NOTE A message is displayed if a quench curv

LS 6000 Scintillation System User’s ManualPN 247971-F 6-16 Isotope/DPM LibrariesSetting Up A Quench Curveentered for each isotope. If the dpm in the s

LS 6000 Scintillation System User’s ManualPN 247971-F 6-17Isotope/DPM LibrariesSetting Up A Quench Curve6in one rack and contain at least five and no

LS 6000 Scintillation System User’s ManualPN 247971-F 1-2 IntroductionGeneral DescriptionConfidence PackThe requires the Productivity Pack and include

LS 6000 Scintillation System User’s ManualPN 247971-F 6-18 Isotope/DPM LibrariesSetting Up A Quench Curve18. The standard data and a quench correlatio

LS 6000 Scintillation System User’s ManualPN 247971-F 6-19Isotope/DPM LibrariesSetting Up A Quench Curve64. Highlight “Review/Edit/Delete Quench Curve

LS 6000 Scintillation System User’s ManualPN 247971-F 6-20 Isotope/DPM LibrariesSetting Up A Quench Curve6. To select the quench curve to edit, highli

LS 6000 Scintillation System User’s ManualPN 247971-F 6-21Isotope/DPM LibrariesSetting Up A Quench Curve67. Highlight “Add or Delete Quench/Efficiency

LS 6000 Scintillation System User’s ManualPN 247971-F 6-22 Isotope/DPM LibrariesSetting Up A Quench Curveappropriate prompts and enter the values. To

LS 6000 Scintillation System User’s ManualPN 247971-F 6-23Isotope/DPM LibrariesSetting Up A Quench Curve61. From the Main Menu, highlight “Isotope/DPM

LS 6000 Scintillation System User’s ManualPN 247971-F 6-24 Isotope/DPM LibrariesSetting Up A Quench Curve4. A prompt at the bottom of the menu allows

LS 6000 Scintillation System User’s ManualPN 247971-F 7-1How Sample Preparation Affects ResultsChemiluminescence77How Sample Preparation Affects Resul

LS 6000 Scintillation System User’s ManualPN 247971-F 7-2 How Sample Preparation Affects ResultsChemiluminescence5. Plant extracts containing chloroph

LS 6000 Scintillation System User’s ManualPN 247971-F 7-3How Sample Preparation Affects ResultsRecognizing And Avoiding Statics7If you are unable to e

LS 6000 Scintillation System User’s ManualPN 247971-F 1-3IntroductionGeneral Description1stepped into position for processing. In turn, each vial is r

LS 6000 Scintillation System User’s ManualPN 247971-F 7-4 How Sample Preparation Affects ResultsCounting Filters And PrecipitatesThis phase problem ca

LS 6000 Scintillation System User’s ManualPN 247971-F 7-5How Sample Preparation Affects ResultsDistinguishing Sample And Instrument Variability7Proced

LS 6000 Scintillation System User’s ManualPN 247971-F 7-6 How Sample Preparation Affects ResultsDistinguishing Sample And Instrument Variability1. The

LS 6000 Scintillation System User’s ManualPN 247971-F 7-7How Sample Preparation Affects ResultsOther Factors That May Affect Accurate Results7Backgrou

LS 6000 Scintillation System User’s ManualPN 247971-F 7-8 How Sample Preparation Affects ResultsOther Factors That May Affect Accurate Results

LS 6000 Scintillation System User’s ManualPN 247971-F a-1Instrument SpecificationsEfficiencyaaInstrument Specificationsa.1 EfficiencyThese specifica

LS 6000 Scintillation System User’s ManualPN 247971-F a-2 Instrument SpecificationsPower Requirementsa.5 Power Requirementsa.6 Dimensionsa.7 Ambient T

LS 6000 Scintillation System User’s ManualPN 247971-F a-3Instrument SpecificationsTemperature Control AccessoryaSet Point must be within 10oC of the

LS 6000 Scintillation System User’s ManualPN 247971-F a-4 Instrument SpecificationsTemperature Control Accessory

LS 6000 Scintillation System User’s ManualPN 247971-F b-1Installation RequirementsElectrical RequirementsbbInstallation RequirementsThis appendix de

LS 6000 Scintillation System User’s ManualPN 247971-F 1-4 IntroductionSpecificationsSystem SetupSystem Setup allows you to set system parameters tailo

LS 6000 Scintillation System User’s ManualPN 247971-F b-2 Installation RequirementsElectrical RequirementsPower lines within the laboratory should pro

LS 6000 Scintillation System User’s ManualPN 247971-F b-3Installation RequirementsSpace Requirementsblines that are separate from those used to supp

LS 6000 Scintillation System User’s ManualPN 247971-F b-4 Installation RequirementsEnvironment Requirements

LS 6000 Scintillation System User’s ManualPN 247971-F c-1RS232SpecificationsccRS232c.1 SpecificationsStandard ASCII format, upper case only, is used

LS 6000 Scintillation System User’s ManualPN 247971-F c-2 RS232RS232 Data OutputWhen XOFF is received, data transmission stops until an XON is receive

LS 6000 Scintillation System User’s ManualPN 247971-F c-3RS232RS232 Data Outputc<Length> is one printable ASCII character (Hex 20 through 7E o

LS 6000 Scintillation System User’s ManualPN 247971-F c-4 RS232RS232 Data OutputHeader message includes a data item giving the type of file. There are

LS 6000 Scintillation System User’s ManualPN 247971-F c-5RS232RS232 Input Modecc.4 RS232 Input ModeThe Input Mode of the LS functions as a remote ke

LS 6000 Scintillation System User’s ManualPN 247971-F c-6 RS232RS232 Input Mode5 sec, Screen SelectionBS Back Space 1 secDL Delete 2 secPrinterPR Prin

LS 6000 Scintillation System User’s ManualPN 247971-F c-7RS232RS232 Input ModecPercent, Window 1110 Requested Counting Precision, RealPercent, Windo

LS 6000 Scintillation System User’s ManualPN 247971-F 1-5IntroductionPrecautions and Limitations1gloves can cause severe static problems which may pro

LS 6000 Scintillation System User’s ManualPN 247971-F c-8 RS232RS232 Input Mode143 SPM: Number Of Data Points Integer144 SPM: Time Per Data Points (Mi

LS 6000 Scintillation System User’s ManualPN 247971-F c-9RS232RS232 Input Modec218 Units Isotope 2 Text (5 Char)219 Units Isotope 3 Text (5 Char)ID

LS 6000 Scintillation System User’s ManualPN 247971-F c-10 RS232RS232 Input Mode314 Replicate Average CPM Coeff. of RealVariation, Percent, Isotope 13

LS 6000 Scintillation System User’s ManualPN 247971-F c-11RS232RS232 Input ModecIsotope 3412 Average Reference Value, Isotope 1RealCoeff, of Variati

LS 6000 Scintillation System User’s ManualPN 247971-F c-12 RS232RS232 Input Mode513 DPM Ratio, Isotope 1 Over Isotope 2Real514 DPM Ratio, Isotope 3 Ov

LS 6000 Scintillation System User’s ManualPN 247971-F c-13RS232RS232 Input Modec537 Xtal DPM Standard Average EfficiencyReal(%)MCA Spectrum DataData

LS 6000 Scintillation System User’s ManualPN 247971-F c-14 RS232RS232 Input Mode905 Current System Status906 User Files (Data 0, .30, or 99 for all)In

LS 6000 Scintillation System User’s ManualPN 247971-F c-15RS232RS232 Input Modecstopped, but counting will continue forthe remaining samples in this

LS 6000 Scintillation System User’s ManualPN 247971-F c-16 RS232RS232 Input Mode170 Beta Norm Multiplier Isotope 1 Real171 Beta Norm Multiplier Isotop

LS 6000 Scintillation System User’s ManualPN 247971-F d-1Isotope Settings and Half-LifeddIsotope Settings and Half-LifeIsotope Setting and Half-Life

LS 6000 Scintillation System User’s ManualPN 247971-F 1-6 IntroductionPrecautions and LimitationsMiniature VialsMiniature Vials within the dimensions

LS 6000 Scintillation System User’s ManualPN 247971-F d-2 Isotope Settings and Half-Life 113Sn-113mIn800 115.1 days-Sn; 99.48 minutes-In125I550 60.25

LS 6000 Scintillation System User’s ManualPN 247971-F d-3Isotope Settings and Half-Lifed0,07 0,9526 0,66 0,6329 1,68 0,3121 4,30 0,05080,08 0,9461 0

LS 6000 Scintillation System User’s ManualPN 247971-F d-4 Isotope Settings and Half-Life 0,36 0,7792 1,24 0,4234 3,10 0,1166 8,40 0,00300,37 0,7738 1,

LS 6000 Scintillation System User’s ManualPN 247971-F d-5Isotope Settings and Half-LifedFigure d.3 Conversion Factors.1 becquerel (Bq) therefore, =

LS 6000 Scintillation System User’s ManualPN 247971-F d-6 Isotope Settings and Half-Life Figure d.5 Iodine-125 Half-Life: 60.25 daysDays0 2 4 6 8 10

LS 6000 Scintillation System User’s ManualPN 247971-F d-7Isotope Settings and Half-Lifed140 0.3293 0.3242 0.3190 0.3140 0.3091 0.3043 0.2994 0.2947

LS 6000 Scintillation System User’s ManualPN 247971-F d-8 Isotope Settings and Half-Life Figure d.8 Carbon-14 Half-Life: 5730 yearsYears0 10 20 30 40

LS 6000 Scintillation System User’s ManualPN 247971-F e-1Radioactive Material LicensingeeRadioactive Material LicensingThe following excerpts from t

LS 6000 Scintillation System User’s ManualPN 247971-F e-2 Radioactive Material Licensing(2) Shall assure that the device is tested for leakage of radi

LS 6000 Scintillation System User’s ManualPN 247971-F e-3Radioactive Material Licensinge(‘1) Shall not export the device containing by-product mater

LS 6000 Scintillation System User’s ManualPN 247971-F 1-7IntroductionHazards1Bio-VialsBio-Vials within the dimensions given on the left are compatible

LS 6000 Scintillation System User’s ManualPN 247971-F e-4 Radioactive Material LicensingRegional USNRC Office and Telephone Numberse.1 Regional USNRC

LS 6000 Scintillation System User’s ManualPN 247971-F e-5Radioactive Material LicensingState Telephone & Address Numbersee.2 State Telephone &am

LS 6000 Scintillation System User’s ManualPN 247971-F e-6 Radioactive Material LicensingState Telephone & Address NumbersConnecticut DirectorMonit

LS 6000 Scintillation System User’s ManualPN 247971-F e-7Radioactive Material LicensingState Telephone & Address NumberseIdaho Radiation Physici

LS 6000 Scintillation System User’s ManualPN 247971-F e-8 Radioactive Material LicensingState Telephone & Address NumbersMaine Nuclear Engineering

LS 6000 Scintillation System User’s ManualPN 247971-F e-9Radioactive Material LicensingState Telephone & Address NumberseMissouri ChiefBureau of

LS 6000 Scintillation System User’s ManualPN 247971-F e-10 Radioactive Material LicensingState Telephone & Address NumbersNew Mexico ChiefBureau o

LS 6000 Scintillation System User’s ManualPN 247971-F e-11Radioactive Material LicensingState Telephone & Address NumberseDirectorBureau of Envi

LS 6000 Scintillation System User’s ManualPN 247971-F e-12 Radioactive Material LicensingState Telephone & Address NumbersPennsylvania DirectorBur

LS 6000 Scintillation System User’s ManualPN 247971-F e-13Radioactive Material LicensingState Telephone & Address NumberseTexas DirectorIndustri

LS 6000 Scintillation System User’s ManualPN 247971-F 1-8 IntroductionHazards2. Contact your Radiation Health and Safety Officer for assistance. Furth

LS 6000 Scintillation System User’s ManualPN 247971-F e-14 Radioactive Material LicensingState Telephone & Address Numbers‘ West Virginia ChiefRad

LS 6000 Scintillation System User’s ManualPN 247971-F 2-1Getting StartedPowering Up22Getting Started2.1 Powering UpThe power switch for the LS is in a

Copyright, Licenses and Trademarks© Beckman Coulter, Inc., 2004. All rights reserved. No part of this publication may be reproduced, transcribed, tran

LS 6000 Scintillation System User’s ManualPN 247971-F 2-2 Getting StartedPowering UpThe only user accessible fuses are the power fuses, located next t

LS 6000 Scintillation System User’s ManualPN 247971-F 2-3Getting StartedPower Failure2WARNING For continued protection against risk of fire, re-place

LS 6000 Scintillation System User’s ManualPN 247971-F 2-4 Getting StartedOperating ControlsThe remaining keys on the keyboard are as follows:Operator

LS 6000 Scintillation System User’s ManualPN 247971-F 2-5Getting StartedOperating Controls2DisplayA monitor is used to display the menus and instructi

LS 6000 Scintillation System User’s ManualPN 247971-F 2-6 Getting StartedOperating Controlsmenus. Below the Main Editing Window is the Data Entry Wind

LS 6000 Scintillation System User’s ManualPN 247971-F 2-7Getting StartedUsing the Racks2Active Key Window. The monitor displays the count data and the

LS 6000 Scintillation System User’s ManualPN 247971-F 2-8 Getting StartedUsing the Racksracks are supplied if Versa-Rack is installed. Bio-Vial racks

LS 6000 Scintillation System User’s ManualPN 247971-F 2-9Getting StartedUsing the Racks2Setting Up the RacksIt is recommended that the Command Cards a

LS 6000 Scintillation System User’s ManualPN 247971-F 2-10 Getting StartedUsing the RacksTo set up the Calibrate Rack, select one of the standard or m

LS 6000 Scintillation System User’s ManualPN 247971-F 2-11Getting StartedPreparing the Printer2To set up the Sample Rack(s), select any of the supplie

Table of ContentsLS 6000 Scintillation System User’s ManualPN 247971-FiSection 1 IntroductionIntended Use . . . . . . . . . . . . . . . . . . . . .

LS 6000 Scintillation System User’s ManualPN 247971-F 2-12 Getting StartedSystem SetupLoading the PaperRefer to the User’s Manual provided with the pr

LS 6000 Scintillation System User’s ManualPN 247971-F 2-13Getting StartedSystem Setup2NOTE System Test is designed for use by a Beckman Coulter Autho

LS 6000 Scintillation System User’s ManualPN 247971-F 2-14 Getting StartedSystem SetupPrinter PagingThe printer sets the top of page based on paper si

LS 6000 Scintillation System User’s ManualPN 247971-F 2-15Getting StartedSystem Setup2RS232The parameters for the RS232 port are selectable based on t

LS 6000 Scintillation System User’s ManualPN 247971-F 2-16 Getting StartedSystem SetupTo change the settings, highlight “Stop Bits” and choose the app

LS 6000 Scintillation System User’s ManualPN 247971-F 2-17Getting StartedSystem Setup2Date/TimeThe current date and time is set at time of installatio

LS 6000 Scintillation System User’s ManualPN 247971-F 2-18 Getting StartedCalibrationTo change these parameters, highlight “AUTO DPM Calibration Setup

LS 6000 Scintillation System User’s ManualPN 247971-F 2-19Getting StartedTemperature Control Accessory2NOTE The unquenched 14C standard must be the f

LS 6000 Scintillation System User’s ManualPN 247971-F 2-20 Getting StartedTemperature Control Accessory

LS 6000 Scintillation System User’s ManualPN 247971-F 3-1Counting SamplesPreparations for Use33Counting Samples3.1 Preparations for UseProvided the po

Table of ContentsLS 6000 Scintillation System User’s ManualPN 247971-FiiStandard Racks (White) . . . . . . . . . . . . . . . . . . . . . . . . . . .

LS 6000 Scintillation System User’s ManualPN 247971-F 3-2 Counting SamplesConducting An Automatic CountYou can load up to 28 standard vial racks or 36

LS 6000 Scintillation System User’s ManualPN 247971-F 3-3Counting SamplesConducting Count Single Rack3NOTE If your samples have already been placed i

LS 6000 Scintillation System User’s ManualPN 247971-F 3-4 Counting SamplesConducting Count Single RackCounting a Single Rack with the Default Paramete

LS 6000 Scintillation System User’s ManualPN 247971-F 3-5Counting SamplesConducting Count Single Rack33. The Main Editing Window prompts you to load y

LS 6000 Scintillation System User’s ManualPN 247971-F 3-6 Counting SamplesConducting Count Single RackTo perform Count Single Rack using a User Progra

LS 6000 Scintillation System User’s ManualPN 247971-F 3-7Counting SamplesConducting Count Single Rack31. With the Main Menu displayed, highlight “Coun

LS 6000 Scintillation System User’s ManualPN 247971-F 3-8 Counting SamplesAuto DPMThe Main Editing Window then prompts you to load your samples and in

LS 6000 Scintillation System User’s ManualPN 247971-F 3-9Counting SamplesMulti-Task3NOTE The Calibrate Rack must contain the unquenched l4~ standard

LS 6000 Scintillation System User’s ManualPN 247971-F 3-10 Counting SamplesMulti-TaskNOTE Multi-Task is automatically terminated if no user action (e

LS 6000 Scintillation System User’s ManualPN 247971-F 3-11Counting SamplesMulti-Task32. From the Multi-Task Menu, highlight “Interrupt Count” and pres

Table of ContentsLS 6000 Scintillation System User’s ManualPN 247971-FiiiSection 3 Counting SamplesPreparations for Use . . . . . . . . . . . . . .

LS 6000 Scintillation System User’s ManualPN 247971-F 3-12 Counting SamplesMulti-TaskNOTE You may abort the Interrupt Count and resume Automatic Coun

LS 6000 Scintillation System User’s ManualPN 247971-F 3-13Counting SamplesMulti-Task3The User Program Review is displayed in the Supplementary Window

LS 6000 Scintillation System User’s ManualPN 247971-F 3-14 Counting SamplesMulti-Taskresults of the Interrupt Count are displayed and stored. Once sto

LS 6000 Scintillation System User’s ManualPN 247971-F 3-15Counting SamplesMulti-Task3To access Interrupt Data:1. From either the Main Menu (Figure 3.1

LS 6000 Scintillation System User’s ManualPN 247971-F 3-16 Counting SamplesMulti-Task3. To print the data, highlight “Print Interrupt Data” and press

LS 6000 Scintillation System User’s ManualPN 247971-F 3-17Counting SamplesMulti-Task3Editing the Current User ProgramOnly the counting time or countin

LS 6000 Scintillation System User’s ManualPN 247971-F 3-18 Counting SamplesMulti-Task7. Press PREVIOUS MENU to return to the Auto Count display.Using

LS 6000 Scintillation System User’s ManualPN 247971-F 3-19Counting SamplesMulti-Task3Isotope Library Section 6 for adding and deleting isotopes if you

LS 6000 Scintillation System User’s ManualPN 247971-F 3-20 Counting SamplesMulti-Task2. From the Multi-Task Menu, highlight “Isotope/DPM Libraries” an

LS 6000 Scintillation System User’s ManualPN 247971-F 4-1Setting Up User ProgramsAbout the User Programs44Setting Up User Programs4.1 About the User P

Table of ContentsLS 6000 Scintillation System User’s ManualPN 247971-FivSection 5 Data CalculationIntroduction . . . . . . . . . . . . . . . . . . .

LS 6000 Scintillation System User’s ManualPN 247971-F 4-2 Setting Up User ProgramsAbout the User ProgramsFigure 4.2 Overview of User ProgramItem Defa

LS 6000 Scintillation System User’s ManualPN 247971-F 4-3Setting Up User ProgramsEditing A User Program4NOTE This section assumes you are familiar wi

LS 6000 Scintillation System User’s ManualPN 247971-F 4-4 Setting Up User ProgramsEditing A User Programthat selection, the allowable responses and th

LS 6000 Scintillation System User’s ManualPN 247971-F 4-5Setting Up User ProgramsEditing A User Program4acceptable, use the Down Cursor key to move to

LS 6000 Scintillation System User’s ManualPN 247971-F 4-6 Setting Up User ProgramsEditing A User ProgramContinue onto the second Review/Edit Menu show

LS 6000 Scintillation System User’s ManualPN 247971-F 4-7Setting Up User ProgramsEditing A User Program4CommentsThe Comments line provides descriptive

LS 6000 Scintillation System User’s ManualPN 247971-F 4-8 Setting Up User ProgramsEditing A User ProgramChoose SPM (if installed) if you want to do si

LS 6000 Scintillation System User’s ManualPN 247971-F 4-9Setting Up User ProgramsEditing A User Program4Edit Other ParametersIf no further editing is

LS 6000 Scintillation System User’s ManualPN 247971-F 4-10 Setting Up User ProgramsEditing A User ProgramTo edit the other parameters, highlight “Edit

LS 6000 Scintillation System User’s ManualPN 247971-F 4-11Setting Up User ProgramsEditing A User Program4Counting PrecisionCounting to a preset counti

Table of ContentsLS 6000 Scintillation System User’s ManualPN 247971-FvLoading Samples for Xtal SL DPM% of Reference . . . . . . . . . . . . . . . .

LS 6000 Scintillation System User’s ManualPN 247971-F 4-12 Setting Up User ProgramsEditing A User ProgramBlanks are samples that are counted at the be

LS 6000 Scintillation System User’s ManualPN 247971-F 4-13Setting Up User ProgramsEditing A User Program4higher energy isotope into the lower energy i

LS 6000 Scintillation System User’s ManualPN 247971-F 4-14 Setting Up User ProgramsEditing A User ProgramPhase MonitorThe 2 Phase Monitor detects and

LS 6000 Scintillation System User’s ManualPN 247971-F 4-15Setting Up User ProgramsEditing A User Program4To change the settings, highlight “Output For

LS 6000 Scintillation System User’s ManualPN 247971-F 4-16 Setting Up User ProgramsEditing A User ProgramFigure 4.10 Menu 2 for Edit Format: CPM.

LS 6000 Scintillation System User’s ManualPN 247971-F 4-17Setting Up User ProgramsEditing A User Program4Figure 4.11 Menu 3 for Edit Format: CPM.Tabl

LS 6000 Scintillation System User’s ManualPN 247971-F 4-18 Setting Up User ProgramsEditing A User ProgramTo select an item to include on the printout,

LS 6000 Scintillation System User’s ManualPN 247971-F 4-19Setting Up User ProgramsCopy User Program4Either Sample or Compton Spectrum, neither spectru

LS 6000 Scintillation System User’s ManualPN 247971-F 4-20 Setting Up User ProgramsCopy User ProgramProgram Section 4. The program copied is still sto

LS 6000 Scintillation System User’s ManualPN 247971-F 5-1Data CalculationIntroduction55Data Calculation5.1 IntroductionThe Data Calculation programs a

Table of ContentsLS 6000 Scintillation System User’s ManualPN 247971-Fvi14C Counting Efficiency . . . . . . . . . . . . . . . . . . . . . . . . . .

LS 6000 Scintillation System User’s ManualPN 247971-F 5-2 Data CalculationCPM/Xtal CPMProcedures for setting up the data calculation programs are pres

LS 6000 Scintillation System User’s ManualPN 247971-F 5-3Data CalculationCPM/Xtal CPM5Half-Life CorrectionSample data can be half-life corrected to th

LS 6000 Scintillation System User’s ManualPN 247971-F 5-4 Data CalculationCPM/Xtal CPMCPM X Factor = Final Answer Printed OutTo change the factor for

LS 6000 Scintillation System User’s ManualPN 247971-F 5-5Data CalculationSL CPM % of Reference/Xtal SL CPM % of Reference5If you are using replicates,

LS 6000 Scintillation System User’s ManualPN 247971-F 5-6 Data CalculationSL CPM % of Reference/Xtal SL CPM % of ReferenceCPM/Xtal CPM Section 5 for i

LS 6000 Scintillation System User’s ManualPN 247971-F 5-7Data CalculationAuto DPM5NOTE Do not leave an empty space for each missing replicate. One em

LS 6000 Scintillation System User’s ManualPN 247971-F 5-8 Data CalculationDPMSetting Up Auto DPMWhen editing a User Program, from the Data Calculation

LS 6000 Scintillation System User’s ManualPN 247971-F 5-9Data CalculationDPM5Single Label DPM uses either IC# or H# Plus (if installed) as the quench

LS 6000 Scintillation System User’s ManualPN 247971-F 5-10 Data CalculationDPMMAIN MENU and refer to Section 6.2 for setting up a quench curve for the

LS 6000 Scintillation System User’s ManualPN 247971-F 5-11Data CalculationXtal DPM5Results for DPMTo count the samples, refer to Section 3.2. A typica

Table of ContentsLS 6000 Scintillation System User’s ManualPN 247971-FviiState Telephone & Address Numbers . . . . . . . . . . . . . . . . . . . .

LS 6000 Scintillation System User’s ManualPN 247971-F 5-12 Data CalculationXtal DPMFigure 5.9 Typical Printout for Dual Label DPM.Figure 5.10 Typica

LS 6000 Scintillation System User’s ManualPN 247971-F 5-13Data CalculationXtal DPM5The Xtalscint DPM program assumes the samples are counting to the s

LS 6000 Scintillation System User’s ManualPN 247971-F 5-14 Data CalculationXtal DPMStandard DateStandard Date is used to correct the dpm of the standa

LS 6000 Scintillation System User’s ManualPN 247971-F 5-15Data CalculationDPM % of Reference5NOTE Do not leave an empty space for each missing replic

LS 6000 Scintillation System User’s ManualPN 247971-F 5-16 Data CalculationXtal SL DPM % of ReferenceSingle and Dual Label DPM % of Reference (if inst

LS 6000 Scintillation System User’s ManualPN 247971-F 5-17Data CalculationXtal SL DPM % of Reference5efficiency. This calculated efficiency is used to

LS 6000 Scintillation System User’s ManualPN 247971-F 5-18 Data CalculationXtal SL DPM % of ReferenceXtal SL DPM % of Reference (if installed) is avai

LS 6000 Scintillation System User’s ManualPN 247971-F 5-19Data CalculationXtal SL DPM % of Reference5If blanks are specified in the User Program as de

LS 6000 Scintillation System User’s ManualPN 247971-F 5-20 Data CalculationSingle Photon MonitoringNOTE Do not leave an empty space for each missing

LS 6000 Scintillation System User’s ManualPN 247971-F 5-21Data CalculationSingle Photon Monitoring5The Counting Time/Sample displayed is entered as th